C₂₆H₂₈N₄O₄

Base Information

Chemical Name:C₂₆H₂₈N₄O₄
CAS No.:1337967-29-9
Molecular Formula:C₂₆H₂₈N₄O₄
Molecular Weight:460.533
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₆H₂₈N₄O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₆H₂₈N₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₆H₂₈N₄O₄

There total 5 articles about C₂₆H₂₈N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353387-36-6
C₂₀H₁₇N₃O₃

: 1337967-29-9
C₂₆H₂₈N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 16 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With lithium hydroxide monohydrate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.109

Reference yield:

: 222986-49-4
methyl 4-(6-aminopyridin-3-yl)benzoate

: 1337967-29-9
C₂₆H₂₈N₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 20 °C

2: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 16 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With lithium hydroxide monohydrate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.109

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1337967-29-9
C₂₆H₂₈N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 16 h / Reflux

2: bis[1,2-bis(diphenylphosphino)ferrocene]-palladium⁽⁰⁾; potassium acetate / dichloromethane; dimethyl sulfoxide / 3 h / 80 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; water; toluene / 5 h / 80 °C

4: tetrahydrofuran / 20 °C

5: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 16 h / 20 °C

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium hydroxide monohydrate; bis[1,2-bis(diphenylphosphino)ferrocene]-palladium⁽⁰⁾; sulfuric acid; potassium acetate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 3: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.07.109