Technology Process of (E)-3-(2-Methoxy-phenyl)-but-2-enoyl azide
There total 4 articles about (E)-3-(2-Methoxy-phenyl)-but-2-enoyl azide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: activated zinc / benzene / Heating
2: 6N hydrochloric acid, acetic acid / Heating
3: potassium hydroxide / ethanol / Heating
4: 1) ethyl chloroformate, triethylamine, 2) sodium azide / 1) acetone, -10 deg C, 2) water, -10 deg C to room temperature
With
hydrogenchloride; potassium hydroxide; sodium azide; chloroformic acid ethyl ester; acetic acid; triethylamine; zinc;
In
ethanol; benzene;
DOI:10.1002/jhet.5570280112
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide / ethanol / Heating
2: 1) ethyl chloroformate, triethylamine, 2) sodium azide / 1) acetone, -10 deg C, 2) water, -10 deg C to room temperature
With
potassium hydroxide; sodium azide; chloroformic acid ethyl ester; triethylamine;
In
ethanol;
DOI:10.1002/jhet.5570280112
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 6N hydrochloric acid, acetic acid / Heating
2: potassium hydroxide / ethanol / Heating
3: 1) ethyl chloroformate, triethylamine, 2) sodium azide / 1) acetone, -10 deg C, 2) water, -10 deg C to room temperature
With
hydrogenchloride; potassium hydroxide; sodium azide; chloroformic acid ethyl ester; acetic acid; triethylamine;
In
ethanol;
DOI:10.1002/jhet.5570280112
