octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one

Base Information

Chemical Name:octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one
CAS No.:75208-81-0
Molecular Formula:C₁₄H₁₇NO₃
Molecular Weight:247.294
Hs Code.:

octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent<e>-1,3-oxazin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one

Chemical Property:

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Technology Process of octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one

There total 3 articles about octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 30212-91-0
3,4-dihydro-3-methyl-4-(2-oxocyclopentyl)-2H-1,3-benzoxazin-2-one

: 75208-81-0
octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one

Guidance literature:: With potassium borohydride; In methanol; for 2h; r.t., overnight;

Reference yield:

: 120-92-3
cyclopentanone

: 75208-81-0
octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / 4-methylbenzenesulfonic acid monohydrate / 2 h / Heating

2: 59 percent / potassium borohydride / methanol / 2 h / r.t., overnight

With potassium borohydride; p-toluenesulfonic acid monohydrate; In methanol;

Reference yield:

: 941-88-8
3,4-dihydro-4-hydroxy-3-methyl-2H-1,3-benzoxazin-2-one

: 75208-81-0
octahydro-4-(2-hydroxyphenyl)-3-methylcyclopent-1,3-oxazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / 4-methylbenzenesulfonic acid monohydrate / 2 h / Heating

2: 59 percent / potassium borohydride / methanol / 2 h / r.t., overnight

With potassium borohydride; p-toluenesulfonic acid monohydrate; In methanol;