3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one

Base Information

• Chemical Name: 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one
• CAS No.: 1252934-13-6
• Molecular Formula: C₄₃H₃₄N₆O₄S₄
• Molecular Weight: 827.045

Synonyms:

Chemical Property of 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one

There total 6 articles about 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

5,5'-[5,5'-methylenebis(3-methylbenzo[b]furan-7,5-diyl)]bis[N-(4-methylbenzylidene)-1,3,4-thiadiazol-2-amine] (1268829-76-0) + mercaptoacetic acid (68-11-1) → 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one (1252934-13-6)

Guidance literature:

With zinc(II) chloride; In N,N-dimethyl-formamide; for 6h; Reflux;

Reference yield: 71.0%

N2-[(E)-1-(4-methylphenyl)methylidene]-5-(3-methyl-5-[3-methyl-7-(5-[(E)-1-(4-methylphenyl)methylidene]amino-1,3,4-thiadiazol-2-yl)benzo[b]furan-5-yl]methylbenzo[b]furan-7-yl)-1,3,4-thiadiazol-2-amine (1252934-03-4) + mercaptoacetic acid (68-11-1) → 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one (1252934-13-6)

Guidance literature:

With zinc(II) chloride; In N,N-dimethyl-formamide; for 6h; Reflux;

DOI:10.1248/cpb.58.805

Reference yield:

C23H22N6O4S2 → 3-(5-3-methyl-5-[(3-methyl-7-5-[2-(4-methylphenyl)-4-oxo-1,3-thiazolan-3-yl]-1,3,4-thiadiazol-2-ylbenzo[b]furan-5-yl)methyl]benzo[b]-furan-7-yl-1,3,4-thiadiazol-2-yl)-2-(4-methylphenyl)-1,3-thiazolan-4-one (1252934-13-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid / 20 °C

2: acetic acid / toluene / 3 h / Reflux

3: zinc(II) chloride / N,N-dimethyl-formamide / 6 h / Reflux

With sulfuric acid; acetic acid; zinc(II) chloride; In N,N-dimethyl-formamide; toluene;

upstream raw materials:

N₂-[(E)-1-(4-methylphenyl)methylidene]-5-(3-methyl-5-[3-methyl-7-(5-[(E)-1-(4-methylphenyl)methylidene]amino-1,3,4-thiadiazol-2-yl)benzo[b]furan-5-yl]methylbenzo[b]furan-7-yl)-1,3,4-thiadiazol-2-amine

mercaptoacetic acid

5-(5-([7-(5-amino-1,3,4-thiadiazol-2-yl)-3-methylbenzo[b]furan-5-yl]methyl)-3-methylbenzo[b]furan-7-yl)-1,3,4-thiadiazol-2-amine

5,5'-[5,5'-methylenebis(3-methylbenzo[b]furan-7,5-diyl)]bis[N-(4-methylbenzylidene)-1,3,4-thiadiazol-2-amine]

Downstream raw materials:

bis(7-{5-[3,5-di(4-methylphenyl)-3,3a-dihydro-2H-pyrazolo[3,4-d]thiazol-6(5H)-yl]-1,3,4-thiadiazol-2-yl}-3-methylbenzofuran-5-yl)methane

3,3'-{5,5'-[5,5'-methylenebis(3-methylbenzo[b]furan-7,5-diyl)]bis(1,3,4-thiadiazole-5,2-diyl)}bis[5-(benzo[d][1,3]dioxol-5-ylmethylene)-2-(4-methylphenyl)thiazolidine-4-one]

3,3'-{5,5'-[5,5'-methylenebis(3-methylbenzo[b]furan-7,5-diyl)]bis(1,3,4-thiadiazole-5,2-diyl)}bis[5-(3-nitrobenzylidene)-2-(4-methylphenyl)thiazolidine-4-one]

3,3'-{5,5'-[5,5'-methylenebis(3-methylbenzo[b]furan-7,5-diyl)]bis(1,3,4-thiadiazole-5,2-diyl)}bis[5-(4-nitrobenzylidene)-2-(4-methylphenyl)thiazolidine-4-one]

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