Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam

Base Information

• Chemical Name: Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam
• CAS No.: 287410-20-2
• Molecular Formula: C₃₇H₄₇N₅O₄*Cu
• Molecular Weight: 689.357

Synonyms:

Chemical Property of Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam

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Technology Process of Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam

There total 1 articles about Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper(II) tetrafluroborate hexahydrate + pyridine-capped centro-(methyl)(benzyloxy)dioxocyclam → Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam (287410-20-2) + Cu(II) complex of centro-(methyl)(benzyloxy)-capped Dioxocyclam*CH2Cl2 (287411-44-3)

Guidance literature:

With K₂CO₃; In dichloromethane; adducts were mixed in pressure tube, tube was capped and the mixt. was heated to 65°C for 2 d; mixt. was filtered, solvent was removed in vac., residue was dissolved in CH2Cl2 and extd. with H2O, water was removed in vac., recrystn. from CH2Cl2/hexane gives two separate products; X-ray diffraction;

DOI:10.1021/ja994352l

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