[Ru(η6-p-cymene)(κ2(S,N)-(N-(2-pyridinyl)amino-diphenylphosphine sulfide)Cl](SbF6)

Base Information

Chemical Name:[Ru(η6-p-cymene)(κ2(S,N)-(N-(2-pyridinyl)amino-diphenylphosphine sulfide)Cl](SbF6)
CAS No.:1258071-46-3
Molecular Formula:C₂₇H₂₉ClN₂PRuS*F₆Sb
Molecular Weight:816.844
Hs Code.:

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Chemical Property of [Ru(η6-p-cymene)(κ2(S,N)-(N-(2-pyridinyl)amino-diphenylphosphine sulfide)Cl](SbF6)

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Technology Process of [Ru(η6-p-cymene)(κ2(S,N)-(N-(2-pyridinyl)amino-diphenylphosphine sulfide)Cl](SbF6)

There total 1 articles about [Ru(η6-p-cymene)(κ2(S,N)-(N-(2-pyridinyl)amino-diphenylphosphine sulfide)Cl](SbF6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 26042-64-8
silver hexafluoroantimonate

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 29938-20-3
N-(2-pyridinyl)amino-diphenylphosphine sulfide

: 1258071-46-3
[Ru(η6-p-cymene)(κ2(S,N)-(N-(2-pyridinyl)amino-diphenylphosphine sulfide)Cl](SbF6)

Guidance literature:: In dichloromethane; byproducts: AgCl; under Ar; to a soln. of Ru-contg. compd. (0.163 mmol) in CH2Cl2 a ligand(0.332 mmol) and Ag-contg. compd. (0.342 mmol) were added and the mixt. was stirred at room temp. for 3 h; AgCl was removed by filtration and the solvent was removed under reducedpressure; the solid was washed with diethyl ether and dried under vac.; elem. anal.;
DOI:10.1016/j.poly.2010.08.014