5,5'-dimethyl-2,2'-bis-3,3'biindole

Base Information

• Chemical Name: 5,5'-dimethyl-2,2'-bis-3,3'biindole
• CAS No.: 118160-28-4
• Molecular Formula: C₄₆H₃₈N₄O₂
• Molecular Weight: 678.833

Synonyms:

Chemical Property of 5,5'-dimethyl-2,2'-bis-3,3'biindole

Chemical Property:

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Technology Process of 5,5'-dimethyl-2,2'-bis-3,3'biindole

There total 2 articles about 5,5'-dimethyl-2,2'-bis-3,3'biindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

3,3-bis(4-methylphenylamino)-1-phenyl-2-propen-1-one (19959-61-6) → 3-benzoyl-5-methyl-2-(4-methylphenylamino)indole (118160-27-3) + 2-(4-methylphenyl)-3-(4-methylphenylimino)-5-phenyl-4-isoxazoline (118160-23-9) + N,N'-bis(4-methylphenyl)-2,2-diacetoxy-3-oxo-3-phenylpropanamidine (118160-26-2) + 5,5'-dimethyl-2,2'-bis-3,3'biindole (118160-28-4)

Guidance literature:

With lead(IV) tetraacetate; In dichloromethane; 1.) -10 deg C - -15 deg C, 5 min; 2.) up to r.t., 3 h;

DOI:10.1016/S0040-4020(01)86728-4

Reference yield: 23.0%

3,3-bis(4-methylphenylamino)-1-phenyl-2-propen-1-one (19959-61-6) → 2-(4-methylphenyl)-3-(4-methylphenylimino)-5-phenyl-4-isoxazoline (118160-23-9) + N,N'-bis(4-methylphenyl)-2,2-diacetoxy-3-oxo-3-phenylpropanamidine (118160-26-2) + 5,5'-dimethyl-2,2'-bis-3,3'biindole (118160-28-4)

Guidance literature:

With lead(IV) tetraacetate; In dichloromethane; 1.) -10 deg C - -15 deg C, 5 min; 2.) up to r.t., 3 h;

DOI:10.1016/S0040-4020(01)86728-4

upstream raw materials:

3,3-bis(4-methylphenylamino)-1-phenyl-2-propen-1-one

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