[Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]

Base Information

Chemical Name:[Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]
CAS No.:917756-94-6
Molecular Formula:C₄₈H₆₉FeN₄
Molecular Weight:757.95
Hs Code.:

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Chemical Property of [Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]

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Technology Process of [Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]

There total 1 articles about [Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3978-81-2
4-tert-butylpyridine

: 917756-93-5
(1-adamantylimido)(2,4-bis(2,6-diisopropylphenylimido)pent-3-yl)iron(III)

: 917756-94-6
[Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]

Guidance literature:: In benzene-d6; NMR tube, toluene-d8, -78°C, Fe-complex, pyridine-compound was added, the tube was shaken; detected by NMR spectra; Kinetics;
DOI:10.1021/ja2005303

Reference yield:

: 917756-94-6
[Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]

: 917756-93-5
(1-adamantylimido)(2,4-bis(2,6-diisopropylphenylimido)pent-3-yl)iron(III)

Guidance literature:: With BPh₃; In benzene-d6; byproducts: 4-t-Bu-pyridine*BPh3; under N2; BPh3 added to Fe complex in C6D6; not isolated; monitored by (1)H NMR spectra;
DOI:10.1021/ic100846b

Reference yield:

: 917756-94-6
[Fe(2,4-bis(2,6-diisopropylphenylimido)pentyl anion)((1-adamantyl)N=)(4-tert-butylpyridine)]

: (i-Pr2C6H3NC(Me)CHC(Me)NC6H3-i-Pr2)Fe(1-adamantyl-NNNN-1-adamantyl-κ2N1,N4)

Guidance literature:: Multi-step reaction with 2 steps

1: BPh₃ / benzene-d6

2: pentane

With BPh₃; In benzene-d6; pentane;
DOI:10.1021/ic100846b