C₆₄H₇₂O₁₀

Base Information

Chemical Name:C₆₄H₇₂O₁₀
CAS No.:1380336-51-5
Molecular Formula:C₆₄H₇₂O₁₀
Molecular Weight:1001.27
Hs Code.:

C<sub>64</sub>H<sub>72</sub>O<sub>10</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₄H₇₂O₁₀

Chemical Property:

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Technology Process of C₆₄H₇₂O₁₀

There total 9 articles about C₆₄H₇₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₂₉H₃₄O₄

: 106-51-4
p-benzoquinone

: 1380336-51-5
C₆₄H₇₂O₁₀

Guidance literature:: In toluene; at 145 ℃; for 96h; Inert atmosphere;
DOI:10.1002/anie.201107765

Reference yield:

: C₁₁H₁₄I₂

: 1380336-51-5
C₆₄H₇₂O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,2-dimethoxyethane; N,N-dimethyl-formamide / 3 h / Inert atmosphere

1.2: 18 h / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; sodium acetate; copper dichloride / tetrahydrofuran / 168 h / 20 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux

4.1: pyridine / 78 h / -30 °C / Inert atmosphere

5.1: potassium tert-butylate / N,N-dimethyl-formamide / 12.5 h / -10 °C / Inert atmosphere

6.1: toluene / 96 h / 145 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; palladium 10% on activated carbon; potassium tert-butylate; sodium acetate; copper dichloride; In tetrahydrofuran; 1,2-dimethoxyethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201107765

Reference yield:

: C₂₇H₃₂O₄

: 1380336-51-5
C₆₄H₇₂O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; sodium acetate; copper dichloride / tetrahydrofuran / 168 h / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux

3: pyridine / 78 h / -30 °C / Inert atmosphere

4: potassium tert-butylate / N,N-dimethyl-formamide / 12.5 h / -10 °C / Inert atmosphere

5: toluene / 96 h / 145 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; palladium 10% on activated carbon; potassium tert-butylate; sodium acetate; copper dichloride; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201107765