9-triphenylphosphinimino-m-carborane

Base Information

Chemical Name:9-triphenylphosphinimino-m-carborane
CAS No.:83679-26-9
Molecular Formula:C₂₀H₂₆B₁₀NP
Molecular Weight:419.517
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Suppliers and Price of 9-triphenylphosphinimino-m-carborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-triphenylphosphinimino-m-carborane

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Technology Process of 9-triphenylphosphinimino-m-carborane

There total 1 articles about 9-triphenylphosphinimino-m-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 84633-96-5
bis-9-M-carboranylbromonium borofluoride

: 83679-26-9
9-triphenylphosphinimino-m-carborane

: 17819-81-7
9-bromo(1,7-dicarba-closo-dodecaborane⁽¹²⁾)

Guidance literature:: With sodium azide; triphenylphosphine; In dichloromethane; water; mixt. of bis(9-m-caboranyl)bromonium borofluoride, NaN3, CH2Cl2, water boiled for 30h; org. layer evapd. to dryness, extn. with heptane, evapn., boiled 6h with P(C6H5)3 in benzene, evapn. in vac., extn. with heptane, 9-m-bromocarborane and P(C6H5)3 sepd., residue dissolved in ether, filtered, evapn., identification by mp.;
DOI:10.1007/BF00953942