Technology Process of C27H24F2N4O2S
There total 7 articles about C27H24F2N4O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane
2: lithium borohydride / tetrahydrofuran
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
4: hydrazine / methanol
5: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl acetamide
With
lithium borohydride; di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; (bis-(2-methoxyethyl)amino)sulfur trufluoride; hydrazine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2012.04.122
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine / methanol
2: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl acetamide
With
N-ethyl-N,N-diisopropylamine; HATU; hydrazine;
In
methanol; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2012.04.122
- Guidance literature:
-
Multi-step reaction with 8 steps
1: palladium on activated charcoal; hydrogen
2: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane
3: Dess-Martin periodane / dichloromethane
4: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane
5: lithium borohydride / tetrahydrofuran
6: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
7: hydrazine / methanol
8: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl acetamide
With
lithium borohydride; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; (bis-(2-methoxyethyl)amino)sulfur trufluoride; hydrazine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2012.04.122