CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2^(2-)*Sm⁽³⁺⁾*OCH(CH₃)2^(1-)=[Sm(CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2)(OCH(CH₃)2)]

Base Information

• Chemical Name: CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2^(2-)*Sm⁽³⁺⁾*OCH(CH₃)2^(1-)=[Sm(CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2)(OCH(CH₃)2)]
• CAS No.: 1156455-07-0
• Molecular Formula: C₃H₇O*C₃₃H₅₁NO₃*Sm
• Molecular Weight: 719.221
• Mol file: 1156455-07-0.mol

Synonyms:

Chemical Property of CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2^(2-)*Sm⁽³⁺⁾*OCH(CH₃)2^(1-)=[Sm(CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2)(OCH(CH₃)2)]

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2^(2-)*Sm⁽³⁺⁾*OCH(CH₃)2^(1-)=[Sm(CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2)(OCH(CH₃)2)]

There total 1 articles about CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2^(2-)*Sm⁽³⁺⁾*OCH(CH₃)2^(1-)=[Sm(CH₃OCH₂CH₂N(CH₂C₆H₂(O)(C(CH₃)3)2)2)(OCH(CH₃)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

CH3OCH2CH2N(CH2C6H2(O)(C(CH3)3)2)2(2-)*Sm(2+)=CH3OCH2CH2N(CH2C6H2(O)(C(CH3)3)2)2Sm + isopropyl alcohol (67-63-0,8013-70-5) → CH3OCH2CH2N(CH2C6H2(O)(C(CH3)3)2)2(2-)*Sm(3+)*OCH(CH3)2(1-)=[Sm(CH3OCH2CH2N(CH2C6H2(O)(C(CH3)3)2)2)(OCH(CH3)2)] (1156455-07-0) + [Sm(CH3OCH2CH2N(CH2C6H2O(C(CH3)3)2)2)2Na(H2O)] (1156455-10-5)

Guidance literature:

In 1,2-dimethoxyethane; byproducts: H2; under N2; excess of i-PrOH added to soln. of Sm-compd. in DME at room temp., stirring overnight; evapn. under vac.; elem. anal.;

DOI:10.1002/zaac.200700442

upstream raw materials:

isopropyl alcohol