C₄₃H₆₀N₈O₁₀S

Base Information

• Chemical Name: C₄₃H₆₀N₈O₁₀S
• CAS No.: 1273327-75-5
• Molecular Formula: C₄₃H₆₀N₈O₁₀S
• Molecular Weight: 881.063
• Mol file: 1273327-75-5.mol

Synonyms:

Chemical Property of C₄₃H₆₀N₈O₁₀S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₃H₆₀N₈O₁₀S

There total 6 articles about C₄₃H₆₀N₈O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C42H55N7O8S → C43H60N8O10S (1273327-75-5)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

2: palladium on activated charcoal; hydrogen / methanol

3: 1-hydroxy-7-aza-benzotriazole; potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium hydrogencarbonate; HATU; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/cbic.201000572

Reference yield:

C48H58N8O12S2 (1273327-69-7) → C43H60N8O10S (1273327-75-5)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate; thiophenol / acetonitrile / 2 h / 20 °C

2: potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

3: palladium on activated charcoal; hydrogen / methanol

4: 1-hydroxy-7-aza-benzotriazole; potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium carbonate; potassium hydrogencarbonate; thiophenol; HATU; In methanol; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/cbic.201000572

Reference yield:

C58H74N8O13S (1273327-66-4) → C43H60N8O10S (1273327-75-5)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol

2: 1-hydroxy-7-aza-benzotriazole; potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium hydrogencarbonate; HATU; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/cbic.201000572

upstream raw materials:

C₄₈H₅₈N₈O₁₂S₂

C₅₈H₇₄N₈O₁₃S

C₂₀H₂₁N₃O₇S

H₂N-Arg(Pbf)-Gly-OBn

Downstream raw materials:

C₂₆H₃₆N₈O₇