4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

Base Information

Chemical Name:4-methoxybenzylthioacetaldehyde sodium bisulfite adduct
CAS No.:85301-94-6
Molecular Formula:C₁₀H₁₃O₅S₂*Na
Molecular Weight:300.332
Hs Code.:

Synonyms:

Suppliers and Price of 4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

There total 3 articles about 4-methoxybenzylthioacetaldehyde sodium bisulfite adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85301-93-5
<<(4-methoxyphenyl)methyl>thio>acetaldehyde

: 85301-94-6
4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

Guidance literature:: With sodium hydrogensulfite; In water; Yield given;
DOI:10.1002/jhet.5570190623

Reference yield:

: 85301-92-4
(2,2-diethoxyethyl)(4-methoxybenzyl)sulfane

: 85301-94-6
4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

Guidance literature:: Multi-step reaction with 2 steps

1: TCA / tetrahydrofuran; H₂O / 48 h

2: NaHSO₃ / H₂O

With sodium hydrogensulfite; trichloroacetic acid; In tetrahydrofuran; water;
DOI:10.1002/jhet.5570190623

Reference yield:

: 6258-60-2
p-methoxybenzylmercaptan

: 85301-94-6
4-methoxybenzylthioacetaldehyde sodium bisulfite adduct

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 72 h / Ambient temperature

2: TCA / tetrahydrofuran; H₂O / 48 h

3: NaHSO₃ / H₂O

With potassium carbonate; sodium hydrogensulfite; trichloroacetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570190623