Technology Process of C24H31NO6S2
There total 7 articles about C24H31NO6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux
2: sodium sulfate / tetrahydrofuran; ethanol / 12 h / 20 °C
3: sodium tetrahydroborate / tetrahydrofuran; ethanol / 4 h / 0 - 20 °C
4: dichloromethane / 0 - 20 °C / Inert atmosphere
5: triethylamine / dichloromethane / 1 h / 0 - 20 °C
6: acetone / 1 h / 20 °C
7: hydrazine hydrochloride; sodium acetate / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
8: hydrogenchloride / ethyl acetate / 3 h / 20 °C / Inert atmosphere
With
hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; hydrazine hydrochloride; sodium acetate; sodium sulfate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/chem.201002964
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dichloromethane / 0 - 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 1 h / 0 - 20 °C
3: acetone / 1 h / 20 °C
4: hydrazine hydrochloride; sodium acetate / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
5: hydrogenchloride / ethyl acetate / 3 h / 20 °C / Inert atmosphere
With
hydrogenchloride; hydrazine hydrochloride; sodium acetate; triethylamine;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/chem.201002964
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium sulfate / tetrahydrofuran; ethanol / 12 h / 20 °C
2: sodium tetrahydroborate / tetrahydrofuran; ethanol / 4 h / 0 - 20 °C
3: dichloromethane / 0 - 20 °C / Inert atmosphere
4: triethylamine / dichloromethane / 1 h / 0 - 20 °C
5: acetone / 1 h / 20 °C
6: hydrazine hydrochloride; sodium acetate / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
7: hydrogenchloride / ethyl acetate / 3 h / 20 °C / Inert atmosphere
With
hydrogenchloride; sodium tetrahydroborate; hydrazine hydrochloride; sodium acetate; sodium sulfate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/chem.201002964