C₂₆H₃₁FN₇O₇P

Base Information

Chemical Name:C₂₆H₃₁FN₇O₇P
CAS No.:1393444-07-9
Molecular Formula:C₂₆H₃₁FN₇O₇P
Molecular Weight:603.547
Hs Code.:

C<sub>26</sub>H<sub>31</sub>FN<sub>7</sub>O<sub>7</sub>P

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₁FN₇O₇P

Chemical Property:

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Technology Process of C₂₆H₃₁FN₇O₇P

There total 9 articles about C₂₆H₃₁FN₇O₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ((2R,3R,4R)-3-(benzoyloxy)-4-fluoro-5-hydroxy-4-methyltetrahydrofuran-2-yl)methyl benzoate

: 1393444-07-9
C₂₆H₃₁FN₇O₇P

Guidance literature:: Multi-step reaction with 8 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / acetonitrile / -40 - 20 °C

2: methanol; ammonia / 110 °C

3: 1H-imidazole

4: toluene-4-sulfonic acid

5: tetrabutyl ammonium fluoride

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / 100 °C

7: tert-butylmagnesium chloride / tetrahydrofuran

8: formic acid / 0 °C

With 1H-imidazole; methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; di-isopropyl azodicarboxylate; tert-butylmagnesium chloride; tetrabutyl ammonium fluoride; ammonia; sodium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile; 1: Mitsunobu reaction / 6: Suzuki coupling;
DOI:10.1016/j.bmc.2012.05.067

Reference yield:

: 874638-93-4
(2R,3R,4R,5R)-5-acetoxy-2-((benzoyloxy)methyl)-4-fluoro-4-methyl-tetrahydrofuran-3-yl benzoate

: 1393444-07-9
C₂₆H₃₁FN₇O₇P

Guidance literature:: Multi-step reaction with 9 steps

1: tributyltin methoxide

2: di-isopropyl azodicarboxylate; triphenylphosphine / acetonitrile / -40 - 20 °C

3: methanol; ammonia / 110 °C

4: 1H-imidazole

5: toluene-4-sulfonic acid

6: tetrabutyl ammonium fluoride

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / 100 °C

8: tert-butylmagnesium chloride / tetrahydrofuran

9: formic acid / 0 °C

With 1H-imidazole; methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; di-isopropyl azodicarboxylate; tert-butylmagnesium chloride; tetrabutyl ammonium fluoride; ammonia; tributyltin methoxide; sodium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile; 2: Mitsunobu reaction / 7: Suzuki coupling;
DOI:10.1016/j.bmc.2012.05.067

Reference yield:

: 913188-90-6
4-amino-7-iodo-1-(2-deoxy-2-fluoro-2-C-methyl-β-D-ribofuranosyl)-1H-pyrrolo[2,3-d]pyrimidine

: 1393444-07-9
C₂₆H₃₁FN₇O₇P

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-imidazole

2: toluene-4-sulfonic acid

3: tetrabutyl ammonium fluoride

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / 100 °C

5: tert-butylmagnesium chloride / tetrahydrofuran

6: formic acid / 0 °C

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; tert-butylmagnesium chloride; tetrabutyl ammonium fluoride; sodium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; water; 4: Suzuki coupling;
DOI:10.1016/j.bmc.2012.05.067