Technology Process of C30H36O8
There total 3 articles about C30H36O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
ethyl acetate;
for 2h;
Heating;
DOI:10.1055/s-0032-1318333
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride; dmap / tetrahydrofuran / 4 h / 0 °C
2: palladium dichloride; copper(l) chloride; oxygen / water; N,N-dimethyl-formamide / 5 h / 20 °C
3: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C
4: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 2 h / Heating
With
dmap; n-butyllithium; oxygen; sodium hydride; diisopropylamine; copper(l) chloride; palladium dichloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; hexane; water; ethyl acetate; N,N-dimethyl-formamide;
2: |Wacker Oxidation / 3: |Aldol Condensation;
DOI:10.1055/s-0032-1318333
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium dichloride; copper(l) chloride; oxygen / water; N,N-dimethyl-formamide / 5 h / 20 °C
2: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 2 h / Heating
With
n-butyllithium; oxygen; diisopropylamine; copper(l) chloride; palladium dichloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; hexane; water; ethyl acetate; N,N-dimethyl-formamide;
1: |Wacker Oxidation / 2: |Aldol Condensation;
DOI:10.1055/s-0032-1318333
