Technology Process of C23H21FN2O2
There total 5 articles about C23H21FN2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene / Reflux
2: palladium 10% on activated carbon; hydrogen / ethanol
3: N-Bromosuccinimide
4: tetrakis(triphenylphosphine) palladium(0); sodium carbonate
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium carbonate;
In
ethanol; toluene;
1: Wittig reaction / 4: Suzuki coupling;
DOI:10.1021/ml200045s
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetic acid
2: trichlorophosphate
3: toluene / Reflux
4: palladium 10% on activated carbon; hydrogen / ethanol
5: N-Bromosuccinimide
6: tetrakis(triphenylphosphine) palladium(0); sodium carbonate
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium carbonate; acetic acid; trichlorophosphate;
In
ethanol; toluene;
2: Vilsmeier formylation / 3: Wittig reaction / 6: Suzuki coupling;
DOI:10.1021/ml200045s
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trichlorophosphate
2: toluene / Reflux
3: palladium 10% on activated carbon; hydrogen / ethanol
4: N-Bromosuccinimide
5: tetrakis(triphenylphosphine) palladium(0); sodium carbonate
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; sodium carbonate; trichlorophosphate;
In
ethanol; toluene;
1: Vilsmeier formylation / 2: Wittig reaction / 5: Suzuki coupling;
DOI:10.1021/ml200045s