1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate

Base Information

• Chemical Name: 1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate
• CAS No.: 1049002-34-7
• Molecular Formula: C₃₂H₂₂BrF₆N₂S₂*NO₃
• Molecular Weight: 754.571

Synonyms:

Chemical Property of 1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate

Chemical Property:

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Technology Process of 1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate

There total 2 articles about 1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromomethyl-4-bromobenzene (589-15-1) + C25H16F6N2S2 (253600-57-6) → 1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate (1049002-34-7)

Guidance literature:

With potassium nitrate; In [D₃]acetonitrile; at 20 ℃; for 168h;

DOI:10.1016/j.tet.2008.05.050

Reference yield:

C32H22BrF6N2S2(1+)*NO3(1-) (1049002-29-0) → 1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate (1049002-34-7)

Guidance literature:

In [D₃]acetonitrile; UV-irradiation;

DOI:10.1016/j.tet.2008.05.050

Reference yield: 97.0%

1-[5'-(pyrid-4''-yl)-2'-methylthien-3'-yl]-2-{2'''-methyl-5'''-[N-(4''''-bromobenzyl-pyrid)-4''''-yl]thien-3'''-yl}perfluorocyclopentene nitrate (1049002-34-7) → C32H22BrF6N2S2(1+)*NO3(1-) (1049002-29-0)

Guidance literature:

In acetonitrile; Irradiation;

DOI:10.1016/j.tet.2008.05.050

upstream raw materials:

C₃₂H₂₂BrF₆N₂S₂⁽¹⁺⁾*NO₃^(1-)

1-bromomethyl-4-bromobenzene

C₂₅H₁₆F₆N₂S₂

Downstream raw materials:

C₃₂H₂₂BrF₆N₂S₂⁽¹⁺⁾*NO₃^(1-)

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