3-O-benzyl-N-demethyldemethoxyoripavine

Base Information

Chemical Name:3-O-benzyl-N-demethyldemethoxyoripavine
CAS No.:86545-95-1
Molecular Formula:C₂₃H₂₁NO₂
Molecular Weight:343.425
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-N-demethyldemethoxyoripavine

Chemical Property:

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Technology Process of 3-O-benzyl-N-demethyldemethoxyoripavine

There total 7 articles about 3-O-benzyl-N-demethyldemethoxyoripavine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86709-01-5
neomorphine

: 86545-95-1
3-O-benzyl-N-demethyldemethoxyoripavine

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent

2: 85 percent / pyridine / 1.) 0 deg C, 2 h, 2.) r.t., 24 h

3: 80 percent / tetrabutylammonium fluoride / acetonitrile / 3 h / Heating

4: 35 percent / sodium ethylate / ethanol / 24 h / Ambient temperature

With pyridine; tetrabutyl ammonium fluoride; sodium ethanolate; In ethanol; acetonitrile;

Reference yield:

: 86680-37-7
3-O-acetylneomorphine

: 86545-95-1
3-O-benzyl-N-demethyldemethoxyoripavine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / pyridine / 1.) 0 deg C, 2 h, 2.) r.t., 24 h

2: 80 percent / tetrabutylammonium fluoride / acetonitrile / 3 h / Heating

3: 35 percent / sodium ethylate / ethanol / 24 h / Ambient temperature

With pyridine; tetrabutyl ammonium fluoride; sodium ethanolate; In ethanol; acetonitrile;

Reference yield:

: 86680-39-9
3-O-acetyl-6-O-mesylneomorphine

: 86545-95-1
3-O-benzyl-N-demethyldemethoxyoripavine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / tetrabutylammonium fluoride / acetonitrile / 3 h / Heating

2: 35 percent / sodium ethylate / ethanol / 24 h / Ambient temperature

With tetrabutyl ammonium fluoride; sodium ethanolate; In ethanol; acetonitrile;