Technology Process of C25H16Cl2F2N6O5
There total 6 articles about C25H16Cl2F2N6O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipotassium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; water;
at 20 ℃;
for 36h;
DOI:10.1016/j.bmcl.2011.09.040
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide; Iodine monochloride / tetrahydrofuran / 4 h / 20 °C
2: dmap; triethylamine / dichloromethane / 0.08 h / 0 °C
3: dipotassium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate; 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 36 h / 20 °C
With
dmap; dipotassium hydrogenphosphate; sodium azide; tetra(n-butyl)ammonium hydrogensulfate; Iodine monochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.09.040
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / 0.08 h / 0 °C
2: dipotassium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate; 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 36 h / 20 °C
With
dmap; dipotassium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; water;
DOI:10.1016/j.bmcl.2011.09.040
