2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile

Base Information

Chemical Name:2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile
CAS No.:960048-18-4
Molecular Formula:C₂₀H₂₁NO
Molecular Weight:291.393
Hs Code.:

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Chemical Property of 2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile

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Technology Process of 2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile

There total 5 articles about 2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200-14-2
4-(n-butyl)benzaldehyde

: 960048-18-4
2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaBH₄ / tetrahydrofuran / 2 h / 0 °C

2: 70 percent / BBr₃ / CH₂Cl₂ / 0.5 h / 0 °C

3: 60 percent / ethanol; H₂O / Heating

4: Na / ethanol / 3 h / Heating

With sodium tetrahydroborate; sodium; boron tribromide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/ol0713990

Reference yield:

: 28788-62-7
4-butylbenzoyl chloride

: 960048-18-4
2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaBH₄ / tetrahydrofuran / 2 h / 0 °C

2: 70 percent / BBr₃ / CH₂Cl₂ / 0.5 h / 0 °C

3: 60 percent / ethanol; H₂O / Heating

4: Na / ethanol / 3 h / Heating

With sodium tetrahydroborate; sodium; boron tribromide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/ol0713990

Reference yield:

: 10531-16-5
p-butylbenzylbromide

: 960048-18-4
2-(4-n-butylphenyl)-3-oxo-4-phenylbutanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / ethanol; H₂O / Heating

2: Na / ethanol / 3 h / Heating

With sodium; In ethanol; water;
DOI:10.1021/ol0713990