C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)

Base Information

Chemical Name:C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)
CAS No.:1448007-93-9
Molecular Formula:BF₄*C₅₀H₃₉NP₃PdS₂
Molecular Weight:1004.14
Hs Code.:

C<sub>50</sub>H<sub>39</sub>NP<sub>3</sub>PdS<sub>2</sub><sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>

Synonyms:

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Chemical Property of C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)

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Technology Process of C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)

There total 5 articles about C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430885-75-8
3-(diphenylphosphino)-1H-indole

: 1448007-93-9
C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: sulfur / toluene / 48 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: acetonitrile / 0.08 h / Inert atmosphere; Schlenk technique; Darkness

3.2: 20 °C / Inert atmosphere; Schlenk technique

4.1: dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With sulfur; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile;
DOI:10.1021/om400464j

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1448007-93-9
C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1.1: methylmagnesium bromide / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere; Schlenk technique

1.2: 20 °C / Inert atmosphere; Schlenk technique

2.1: triethylamine / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere; Schlenk technique

2.2: 1 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: sulfur / toluene / 48 h / 20 °C / Inert atmosphere; Schlenk technique

4.1: acetonitrile / 0.08 h / Inert atmosphere; Schlenk technique; Darkness

4.2: 20 °C / Inert atmosphere; Schlenk technique

5.1: dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With sulfur; methylmagnesium bromide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile;
DOI:10.1021/om400464j

Reference yield:

: 1430885-76-9
1,3-bis(diphenylphosphino)-1H-indole

: 1448007-93-9
C₅₀H₃₉NP₃PdS₂⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfur / toluene / 48 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: acetonitrile / 0.08 h / Inert atmosphere; Schlenk technique; Darkness

2.2: 20 °C / Inert atmosphere; Schlenk technique

3.1: dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With sulfur; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/om400464j