acacen[B(Ph)-O-B(Ph)]

Base Information

• Chemical Name: acacen[B(Ph)-O-B(Ph)]
• CAS No.: 682355-81-3
• Molecular Formula: C₂₄H₂₈B₂N₂O₃
• Molecular Weight: 414.12
• Mol file: 682355-81-3.mol

Synonyms:

Chemical Property of acacen[B(Ph)-O-B(Ph)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acacen[B(Ph)-O-B(Ph)]

There total 1 articles about acacen[B(Ph)-O-B(Ph)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

N,N'-ethylenebis(4-iminopentan-2-one) (7275-44-7,56570-48-0) + phenylboronic acid (98-80-6) → acacen[B(Ph)-O-B(Ph)] (682355-81-3,682809-53-6)

Guidance literature:

In benzene; acacenH2 and PhB(OH)2 (1:2) in benzene were refluxed for 1 h with Dean-Stark trap; react. mixt. was cooled to room temp., ppt. was filtered off under vac. and washed with benzene; elem. anal.;

DOI:10.1016/j.jorganchem.2003.11.032

Reference yield: 58.0%

acacen[B(Ph)-O-B(Ph)] (682355-81-3,682809-53-6) + water (7732-18-5) → (CH3COCHC(CH3)NHCH2CH2NH2)(BOC6H5)3*0.5(CH3COCHC(CH3)NHCH2)2

Guidance literature:

In benzene; crystn. from benzene; elem. anal.;

DOI:10.1016/j.jorganchem.2003.11.032

upstream raw materials:

N,N'-ethylenebis(4-iminopentan-2-one)

phenylboronic acid