C₁₁H₁₇NO₄

Base Information

• Chemical Name: C₁₁H₁₇NO₄
• CAS No.: 1453315-97-3
• Molecular Formula: C₁₁H₁₇NO₄
• Molecular Weight: 227.26

Synonyms:

Chemical Property of C₁₁H₁₇NO₄

Chemical Property:

• Melting Point: 63-68°C

Purity/Quality:

99%, ^*data from raw suppliers

2-Boc-8-oxo-5-oxa-2-azaspiro[3.4]octane 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₇NO₄

There total 3 articles about C₁₁H₁₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C12H19NO4 (1453315-95-1) → C11H17NO4 (1453315-97-3)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; at 0 - 20 ℃; for 0.833333h; Inert atmosphere;

DOI:10.1021/ol402127b

Reference yield:

tert-butyl 3-oxoazetidine-1-carboxylate (398489-26-4) → C11H17NO4 (1453315-97-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 °C / Inert atmosphere

2.1: potassium tert-butylate; perhydrodibenzo-18-crown-6 / tert-butyl alcohol / 9 h / Inert atmosphere; Reflux

3.1: toluene-4-sulfonic acid / acetone / 0.83 h / 0 - 20 °C / Inert atmosphere

With perhydrodibenzo-18-crown-6; n-butyllithium; potassium tert-butylate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; acetone; tert-butyl alcohol;

DOI:10.1021/ol402127b

Reference yield:

C12H19NO4 (1453315-93-9) → C11H17NO4 (1453315-97-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium tert-butylate; perhydrodibenzo-18-crown-6 / tert-butyl alcohol / 9 h / Inert atmosphere; Reflux

2: toluene-4-sulfonic acid / acetone / 0.83 h / 0 - 20 °C / Inert atmosphere

With perhydrodibenzo-18-crown-6; potassium tert-butylate; toluene-4-sulfonic acid; In acetone; tert-butyl alcohol;

DOI:10.1021/ol402127b

upstream raw materials:

tert-butyl 3-oxoazetidine-1-carboxylate

C₁₂H₁₉NO₄

C₁₂H₁₉NO₄

Downstream raw materials:

C₁₁H₁₉NO₄

C₁₁H₂₀N₂O₃

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