C₂₇H₃₂O₈

Base Information

Chemical Name:C₂₇H₃₂O₈
CAS No.:1600522-75-5
Molecular Formula:C₂₇H₃₂O₈
Molecular Weight:484.546
Hs Code.:

C<sub>27</sub>H<sub>32</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₇H₃₂O₈

There total 4 articles about C₂₇H₃₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428369-20-3
C₁₄H₂₂O₄

: 1600522-75-5
C₂₇H₃₂O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.17 h / -78 °C / Inert atmosphere

2.1: tetrahydrofuran / 15.5 h / -78 - 20 °C / Inert atmosphere

3.1: potassium carbonate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride / 1 h / 0 - 40 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201308824

Reference yield:

: 1600522-69-7
C₂₂H₃₄O₆Si

: 1600522-75-5
C₂₇H₃₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride / 1 h / 0 - 40 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine; In methanol;
DOI:10.1002/anie.201308824

Reference yield:

: C₁₆H₂₄O₆

: 1600522-75-5
C₂₇H₃₂O₈

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 15.5 h / -78 - 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

3: triethylamine; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride / 1 h / 0 - 40 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201308824