mer-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}(sulfur dioxide)molybdenum

Base Information

• Chemical Name: mer-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}(sulfur dioxide)molybdenum
• CAS No.: 121314-13-4
• Molecular Formula: C₅₃H₄₄As₂MoO₅P₂S
• Molecular Weight: 1100.73
• Mol file: 121314-13-4.mol

Synonyms:

Chemical Property of mer-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}(sulfur dioxide)molybdenum

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of mer-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}(sulfur dioxide)molybdenum

There total 1 articles about mer-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}(sulfur dioxide)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

fac-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}molydenum (121289-43-8) → mer-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}(sulfur dioxide)molybdenum (121314-13-4)

Guidance literature:

With sulfur dioxide; In dichloromethane; SO2 reacts in CH2Cl2 with (CO)3Mo(Ph2PCH2AsPh2)2 at 20°C (O.5 h), reduced the soln. in vacuo, addn. of hexane at -20°C, (CO)3(SO2)Mo(Ph2PCH2AsPh2)2 is crystallized; product is filtered, washed with hexane and dried in vacuo, elem. anal.;

upstream raw materials:

fac-tricarbonylbis{((diphenylarsino)methyl)diphenylphosphane}molydenum