Technology Process of 1,2-Dihydrocyclobuta[b]quinoline
There total 7 articles about 1,2-Dihydrocyclobuta[b]quinoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver carbonate;
In
1,4-dioxane;
at 140 ℃;
for 24h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/adsc.201700509
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / tetrahydrofuran / 20 °C
2: pyridinium chlorochromate / dichloromethane / 20 °C
3: sodium hydride / tetrahydrofuran / 80 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 80 °C
5: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 20 °C
6: silver carbonate / 1,4-dioxane / 24 h / 140 °C / Inert atmosphere; Schlenk technique
With
tetrabutyl ammonium fluoride; tetrabutylammomium bromide; sodium hydride; potassium carbonate; silver carbonate; pyridinium chlorochromate; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/adsc.201700509
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridinium chlorochromate / dichloromethane / 20 °C
2: sodium hydride / tetrahydrofuran / 80 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 80 °C
4: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 20 °C
5: silver carbonate / 1,4-dioxane / 24 h / 140 °C / Inert atmosphere; Schlenk technique
With
tetrabutyl ammonium fluoride; tetrabutylammomium bromide; sodium hydride; silver carbonate; pyridinium chlorochromate; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/adsc.201700509
