C₂₉H₃₆N₂O₆

Base Information

Chemical Name:C₂₉H₃₆N₂O₆
CAS No.:1419075-27-6
Molecular Formula:C₂₉H₃₆N₂O₆
Molecular Weight:508.615
Hs Code.:

C<sub>29</sub>H<sub>36</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₆N₂O₆

Chemical Property:

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Technology Process of C₂₉H₃₆N₂O₆

There total 10 articles about C₂₉H₃₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1419075-32-3
benzyl (7S,8S,10R)-7-[(1,3-dioxoisoindolin-2-yl)methyl]-10-methyl-8-propyl-1,5-dioxa-9-azaspiro[5.5]undecane-9-carboxylate

: 1419075-27-6
C₂₉H₃₆N₂O₆

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at -20 - 5 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/ejoc.201200919

Reference yield:

: 1350922-84-7
(R)-benzyl [1-(2-(2-aminoethyl)-1,3-dioxan-2-yl)propan-2-yl]carbamate

: 1419075-27-6
C₂₉H₃₆N₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

3.1: magnesium sulfate / dichloromethane / Reflux

3.2: 14 h / 40 °C

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

5.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

6.1: Amberlite IRA 401 / methanol

7.1: triethylamine / toluene / 3 h / Dean-Stark; Reflux

8.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / -20 - 5 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; palladium 10% on activated carbon; ammonium formate; sodium carbonate; magnesium sulfate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 3.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919

Reference yield:

: (R)-benzyl [1-(2-(2-(1,3-dioxoisoindolin-2-yl)ethyl)-1,3-dioxan-2-yl)propan-2-yl]carbamate

: 1419075-27-6
C₂₉H₃₆N₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrazine hydrate / methanol / 2 h / Reflux

2.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.2: 0.5 h / 0 - 20 °C

3.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

4.1: magnesium sulfate / dichloromethane / Reflux

4.2: 14 h / 40 °C

5.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

6.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

7.1: Amberlite IRA 401 / methanol

8.1: triethylamine / toluene / 3 h / Dean-Stark; Reflux

9.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / -20 - 5 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; palladium 10% on activated carbon; ammonium formate; sodium carbonate; magnesium sulfate; hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 4.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919