Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate

Base Information

Chemical Name:Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate
CAS No.:132561-48-9
Molecular Formula:C₃₈H₄₇N₅O₆
Molecular Weight:669.821
Hs Code.:

Methyl (3S,4S)-4-<N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidyl>amino-3-hydroxy-6-methylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate

Chemical Property:

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Technology Process of Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate

There total 5 articles about Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: (S)-3-(1H-Imidazol-4-yl)-2-[(R)-3-naphthalen-1-yl-2-(phenethylcarbamoyl-methyl)-propionylamino]-propionyl azide

: 132561-48-9
Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3042

Reference yield:

: 132488-68-7
N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

: 132561-48-9
Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / hydrazine hydrate / methanol / overnight

2: isoamyl nitrite

3: 16 percent / Et₃N / dimethylformamide

With hydrazine hydrate; triethylamine; isopentyl nitrite; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3042

Reference yield:

: 105227-75-6
N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

: 132561-48-9
Methyl (3S,4S)-4--L-histidyl>amino-3-hydroxy-6-methylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: isoamyl nitrite

2: 16 percent / Et₃N / dimethylformamide

With triethylamine; isopentyl nitrite; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3042