C₅₈H₇₄O₁₀

Base Information

Chemical Name:C₅₈H₇₄O₁₀
CAS No.:138268-06-1
Molecular Formula:C₅₈H₇₄O₁₀
Molecular Weight:931.22
Hs Code.:

C<sub>58</sub>H<sub>74</sub>O<sub>10</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₈H₇₄O₁₀

Chemical Property:

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Technology Process of C₅₈H₇₄O₁₀

There total 7 articles about C₅₈H₇₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 138268-03-8,138268-04-9
C₆₀H₇₆O₁₁

: 138268-06-1
C₅₈H₇₄O₁₀

Guidance literature:: With sodium hydroxide; for 20h; Ambient temperature;
DOI:10.1248/cpb.39.2333

Reference yield:

: 35906-40-2
methyl 3,4-di-O-acetyl-α-D-glucuronatopyranose exo-1,2-O-(ethyl orthoacetate)

: 138268-06-1
C₅₈H₇₄O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: 38 g / ammonia saturated MeOH / methanol / 20 h / Ambient temperature

2: 15.3 g / silver oxide / dimethylformamide / 20 h / Ambient temperature

3: 83 percent / 95percent aq. acetic acid / 0.25 h / Ambient temperature

4: 48 percent / pyridine / Ambient temperature

5: 16 percent / trimethylsilyl trifluoromethanesulfonate, molecular sieve (4 Angstroem) / CH₂Cl₂ / 48 h / 50 °C

6: 86 percent / methanolic NaOH / 20 h / Ambient temperature

With pyridine; sodium hydroxide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; ammonia; acetic acid; silver(l) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.2333

Reference yield:

: (3aR,5S,6S,7S,7aR)-2-Ethoxy-6,7-dihydroxy-2-methyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran-5-carboxylic acid; compound with ammonia

: 138268-06-1
C₅₈H₇₄O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: 15.3 g / silver oxide / dimethylformamide / 20 h / Ambient temperature

2: 83 percent / 95percent aq. acetic acid / 0.25 h / Ambient temperature

3: 48 percent / pyridine / Ambient temperature

4: 16 percent / trimethylsilyl trifluoromethanesulfonate, molecular sieve (4 Angstroem) / CH₂Cl₂ / 48 h / 50 °C

5: 86 percent / methanolic NaOH / 20 h / Ambient temperature

With pyridine; sodium hydroxide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; acetic acid; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.39.2333