(C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄

Base Information

Chemical Name:(C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄
CAS No.:86731-38-6
Molecular Formula:AlCl₄*C₁₈H₁₇Fe
Molecular Weight:457.974
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)Fe(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*AlCl<sub>4</sub><sup>(1-)</sup>=((C<sub>5</sub>H<sub>5</sub>)Fe(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>))AlCl<sub>4</sub>

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Chemical Property of (C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄

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Technology Process of (C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄

There total 1 articles about (C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-54-5,55404-68-7
ferrocene

: 101-81-5
Diphenylmethane

: 86731-38-6
(C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄

Guidance literature:: With aluminium trichloride; aluminium; In cyclohexane; a mixt. of FcH, AlCl, Al powder, and Ph2CH2 in 5/10/8/15 ratio was heated under reflux in cyclohexane at 82°C for 10 h under N2; the reaction mixt. was hydroloyzed with ice cold water, aq. phase was washed with ether; not isolated from the soln.;
DOI:10.1016/S0022-328X(00)98831-4

Reference yield:

: ammonium hexafluorophosphate

: 86731-38-6
(C₅H₅)Fe(C₆H₅CH₂C₆H₅)⁽¹⁺⁾*AlCl₄^(1-)=((C₅H₅)Fe(C₆H₅CH₂C₆H₅))AlCl₄

: (η(5)-cyclopentadienyl)[(1,2,2,3,3,4-η(6))-benzophenone]iron(II) hexafluorophosphate

Guidance literature:: With potassium permanganate; In water; byproducts: MnO2; an aq. soln. of AlCl4(1-) salt was added to aq. KMnO4, mixt. was heatedfor 10 h at 60°C, stirred for 10 h, filtered through Celite, aq.NH4PF6 was added; yield 20% (including previous reaction of ferrocene with Ph2CH2 and Al/AlCl3); ppt. was recrystd. from acetone/Et2O; elem. anal.;
DOI:10.1016/S0022-328X(00)98831-4