1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene

Base Information

• Chemical Name: 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene
• CAS No.: 110434-38-3
• Molecular Formula: C₂₀H₂₅ClO
• Molecular Weight: 316.871
• Mol file: 110434-38-3.mol

Synonyms:

Chemical Property of 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene

There total 3 articles about 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methyl-1-pentene (763-29-1) + 4-methoxybenzhydryl chloride (6731-11-9) → 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene (110434-38-3)

Guidance literature:

With boron trichloride; Thermodynamic data; Rate constant; 1) CH2Cl2, 2) CH2Cl2, -70 deg C; investigations of reaction: carbenium ios, 2-methyl-1-pentene, variation of educt-conc., kinetics, ΔH(excit.), ΔS(excit.), ΔG(excit.), influence of subst. to reactivity;

Reference yield:

2-Methyl-1-pentene (763-29-1) + p-methoxydiphenylcarbenium tetrachloroborate → 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene (110434-38-3)

Guidance literature:

In dichloromethane; at -70 - -30 ℃; for 2h; Rate constant; Thermodynamic data; ΔH(excit.), ΔS(excit.);

DOI:10.1021/jo00080a027

Reference yield:

2-Methyl-1-pentene (763-29-1) → 1-(3-Chloro-3-methyl-1-phenyl-hexyl)-4-methoxy-benzene (110434-38-3) + C21H27ClO (110434-39-4)

Guidance literature:

With boron trichloride; In dichloromethane; at -70 ℃; competition reaction with diarylmethyl chloride (1a) and diarylmethyl chloride (1b); relative reactivity in dependence on concentration of BCl₃;

upstream raw materials:

2-Methyl-1-pentene

4-methoxybenzhydryl chloride