C₃₄H₃₉N₃O₇

Base Information

• Chemical Name: C₃₄H₃₉N₃O₇
• CAS No.: 1416792-18-1
• Molecular Formula: C₃₄H₃₉N₃O₇
• Molecular Weight: 601.7
• Mol file: 1416792-18-1.mol

Synonyms:

Chemical Property of C₃₄H₃₉N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₉N₃O₇

There total 3 articles about C₃₄H₃₉N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

C20H24N3O4(1+)*C2F3O2(1-) + 3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid (40662-29-1) → C34H39N3O7 (1416792-18-1)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; for 12h; Inert atmosphere;

DOI:10.1021/ja309346f

Reference yield:

N-butyl-4-amino-1,8-naphthalimide (55490-98-7) → C34H39N3O7 (1416792-18-1)

Guidance literature:

Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 20 h / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

3: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja309346f

Reference yield:

4-amino-1,8-naphthalic anhydride (6492-86-0) → C34H39N3O7 (1416792-18-1)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol / 14 h / Inert atmosphere; Reflux

2: N,N-dimethyl-formamide / 20 h / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

4: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja309346f

upstream raw materials:

3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid

N-butyl-4-amino-1,8-naphthalimide

4-amino-1,8-naphthalic anhydride