C₂₅H₃₁FN₄O₅S

Base Information

Chemical Name:C₂₅H₃₁FN₄O₅S
CAS No.:1417392-20-1
Molecular Formula:C₂₅H₃₁FN₄O₅S
Molecular Weight:518.609
Hs Code.:

C<sub>25</sub>H<sub>31</sub>FN<sub>4</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₅H₃₁FN₄O₅S

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Technology Process of C₂₅H₃₁FN₄O₅S

There total 9 articles about C₂₅H₃₁FN₄O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1417497-97-2
C₂₀H₂₃FN₄O₃S

: 1417392-20-1
C₂₅H₃₁FN₄O₅S

Guidance literature:: With triethylamine; In dichloromethane; at 23 ℃; for 2h;
DOI:10.1021/jm301626p

Reference yield:

: 39122-97-9
2-benzyl-6-methyl-2,6-diazatricyclo[3.3.1.1^3,7]decane

: 1417392-20-1
C₂₅H₃₁FN₄O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium on activated charcoal / methanol / 4 h / 60 °C

2: caesium carbonate / acetonitrile / 1 h / 180 °C / Irradiation

3: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 2.17 h / 0 °C / Reflux

4: triethylamine / dichloromethane / 2 h / 23 °C

With carbonochloridic acid 1-chloro-ethyl ester; palladium on activated charcoal; hydrogen; caesium carbonate; triethylamine; In methanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jm301626p

Reference yield:

: 49738-67-2
C₁₆H₂₃BrN₂

: 1417392-20-1
C₂₅H₃₁FN₄O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / water / 0.5 h / 65 - 70 °C

2.1: N-chloro-succinimide / diethyl ether / 0.22 h / 23 °C / Inert atmosphere

2.2: 0.83 h / Inert atmosphere; Irradiation

3.1: hydrogen; palladium on activated charcoal / methanol / 4 h / 60 °C

4.1: caesium carbonate / acetonitrile / 1 h / 180 °C / Irradiation

5.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 2.17 h / 0 °C / Reflux

6.1: triethylamine / dichloromethane / 2 h / 23 °C

With N-chloro-succinimide; carbonochloridic acid 1-chloro-ethyl ester; sulfuric acid; palladium on activated charcoal; hydrogen; caesium carbonate; triethylamine; In methanol; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; 2.1: |Hofmann-Loeffler-Freytag Synthesis / 2.2: |Hofmann-Loeffler-Freytag Synthesis;
DOI:10.1021/jm301626p