WCl₄(O-2,6-C₆H₃Cl₂)2

Base Information

Chemical Name:WCl₄(O-2,6-C₆H₃Cl₂)2
CAS No.:95340-20-8
Molecular Formula:C₁₂H₆Cl₈O₂W
Molecular Weight:649.652
Hs Code.:

WCl<sub>4</sub>(O-2,6-C<sub>6</sub>H<sub>3</sub>Cl<sub>2</sub>)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of WCl₄(O-2,6-C₆H₃Cl₂)2

Chemical Property:

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Technology Process of WCl₄(O-2,6-C₆H₃Cl₂)2

There total 1 articles about WCl₄(O-2,6-C₆H₃Cl₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 87-65-0
2,6-Dichlorophenol

: 13283-01-7
tungsten(VI) chloride

: 95340-20-8,111465-11-3
WCl₄(O-2,6-C₆H₃Cl₂)2

Guidance literature:: In tetrachloromethane; addn. of soln. of 2,6-Cl2C6H3OH in CCl4 to WCl6 suspended in CCl4 (Ar-atmosphere); stirring under reflux for 4 h;; removing solvent and washing with ethanol; elem. anal.;;

Reference yield:

: 67608-37-1
Mg(CH₂C(CH₃)3)2 * dioxane

: 95340-20-8,111465-11-3
WCl₄(O-2,6-C₆H₃Cl₂)2

: W(OC₆H₃Cl₂)2Cl₂(CHC(CH₃)3)(O(C₂H₅)2)

Guidance literature:: In diethyl ether; byproducts: MgCl2(dioxane), neopentane; 1 h at 25°C, 1 equiv. of Mg-compound; decanted; filtered; evapd.;
DOI:10.1039/c39850001816

Reference yield:

: 67608-37-1
Mg(CH₂C(CH₃)3)2 * dioxane

: 95340-20-8,111465-11-3
WCl₄(O-2,6-C₆H₃Cl₂)2

: 103352-29-0
W(OC₆H₃Cl₂)2Cl(CH₂C(CH₃)3)(CHC(CH₃)3)(O(C₂H₅)2)

Guidance literature:: In diethyl ether; byproducts: MgCl2(dioxane), neopentane; room temp., 1.5 equiv. of Mg-compound; decanted; filtered; evapd.;
DOI:10.1039/c39850001816