benzyldicyclopentadienyllutetium-tetrahydrofuran (1/1)

Base Information

• Chemical Name: benzyldicyclopentadienyllutetium-tetrahydrofuran (1/1)
• CAS No.: 76207-11-9
• Molecular Formula: C₄H₈O*C₁₇H₁₇Lu
• Molecular Weight: 468.396

Synonyms:

Chemical Property of benzyldicyclopentadienyllutetium-tetrahydrofuran (1/1)

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Technology Process of benzyldicyclopentadienyllutetium-tetrahydrofuran (1/1)

There total 1 articles about benzyldicyclopentadienyllutetium-tetrahydrofuran (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

lutetium(III) chloride (10099-66-8) + benzyllithium*2THF + sodium cyclopentadienide → benzyldicyclopentadienyllutetium-tetrahydrofuran (1/1) (76207-11-9)

Guidance literature:

In tetrahydrofuran; pentane; byproducts: NaCl; To a suspn. of LuCl3 in THF at room temp. was added a soln. of NaC5H5 in THF, the mixt. was stirred for 2 h and cooled to -78°C, a soln.of RLi in pentane was added, stirred for 6 h at -78°C, warmed toroom temp. (Ar atm.);; evapd., ppt. was extd. with toluene, evapd., ppt. was washed with pentane-Et2O, filtered, dried; elem. anal.;;

upstream raw materials:

lutetium(III) chloride

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