trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium

Base Information

Chemical Name:trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium
CAS No.:1310457-91-0
Molecular Formula:C₆₈H₈₃ClO₂P₂Pd
Molecular Weight:1136.23
Hs Code.:

Synonyms:

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Chemical Property of trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium

Chemical Property:

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Technology Process of trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium

There total 1 articles about trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 52522-40-4
tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex

: 1310421-10-3
3,5-didodecyl-2,6-diformylphenyl trifluoromethanesulfonate

: 603-35-0
triphenylphosphine

: lithium chloride

: 1310457-91-0
trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium

Guidance literature:: In dichloromethane; (N2); stirring soln. of palladium compd., aldehyde deriv. and triphenylphosphine in anhyd. CH2Cl2 at 25°C for 39 h, evapn., addn. of LiCl, dissolving in acetone and water, stirring at 25°C for 24 h; extn. (CHCl3), washing with water, drying over Na2SO4, evapn., chromy. (silica gel, CHCl3), elem. anal.;
DOI:10.1039/c1dt10556f

Reference yield: 76.0%

: 1333471-40-1
4-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]methylaniline

: 1310457-91-0
trans-(3,5-didodecyl-2,6-diformylphenyl)chlorobis(triphenylphosphine)palladium

: 1310457-78-3
(3,5-dodecyl-2,6-bis(N-4-(2,5,8,11-tetraoxadecyl)phenylimino)phenyl)chloropalladium

Guidance literature:: With (H₂N)2CO*H₂O₂; In acetonitrile; (N2); refluxing soln. of palladium compd. and aniline deriv. in anhyd. CH3CN for 86 h, cooling ot 25°C, addn. of urea hydrogen peroxide, stirring at 50°C for 24 h; evapn., chromy. (silica gel, 1-2% methanol/CHCl3), gel permeation chromy. (CHCl3), elem. anal.;
DOI:10.1039/c1dt10556f