C₁₈H₂₄O₆

Base Information

Chemical Name:C₁₈H₂₄O₆
CAS No.:1323316-45-5
Molecular Formula:C₁₈H₂₄O₆
Molecular Weight:336.385
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₄O₆

Chemical Property:

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Technology Process of C₁₈H₂₄O₆

There total 9 articles about C₁₈H₂₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₆O₈

: 1323316-45-5
C₁₈H₂₄O₆

Guidance literature:: With hydrogenchloride; In methanol; water; at 40 ℃; for 6h;
DOI:10.1021/ml200067t

Reference yield:

: 946063-58-7
N-methoxy-N-methyl-3-((4S,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)propanamide

: 1323316-45-5
C₁₈H₂₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

1.2: 0.25 h / -78 °C

2.1: Hoveyda-Grubbs catalyst second generation / 1,2-dichloro-ethane / 1 h / Reflux

3.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 20 h / 20 °C

5.1: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 16 h / Reflux

7.1: hydrogenchloride / methanol; water / 6 h / 40 °C

With hydrogenchloride; dmap; sodium tetrahydroborate; Hoveyda-Grubbs catalyst second generation; palladium 10% on activated carbon; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ml200067t

Reference yield:

: 946063-57-6
(S)-pent-4-en-2-yl 2,4-bis(methoxymethoxy)-6-(4-((4S,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)-2-oxobutyl)benzoate

: 1323316-45-5
C₁₈H₂₄O₆

Guidance literature:: Multi-step reaction with 6 steps

1: Hoveyda-Grubbs catalyst second generation / 1,2-dichloro-ethane / 1 h / Reflux

2: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

3: palladium 10% on activated carbon; hydrogen / ethanol / 20 h / 20 °C

4: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C

5: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 16 h / Reflux

6: hydrogenchloride / methanol; water / 6 h / 40 °C

With hydrogenchloride; dmap; sodium tetrahydroborate; Hoveyda-Grubbs catalyst second generation; palladium 10% on activated carbon; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ml200067t