3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate

Base Information

• Chemical Name: 3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate
• CAS No.: 173347-57-4
• Molecular Formula: C₂₂H₁₅Br₂N₂*ClO₄
• Molecular Weight: 566.633
• Mol file: 173347-57-4.mol

Synonyms:

Chemical Property of 3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate

There total 2 articles about 3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[5-Bromo-2-(3-imino-3,4-dihydro-1H-isoquinolin-2-yl)-phenyl]-(4-bromo-phenyl)-methanone; hydrobromide → 3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate (173347-57-4)

Guidance literature:

With perchloric acid; In acetic acid; for 0.166667h; Heating;

DOI:10.1007/BF01166335

Reference yield:

(2-bromomethylphenyl)acetonitrile (73217-11-5) → 3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate (173347-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 12 h / Heating

2: 70percent HClO₄ / acetic acid / 0.17 h / Heating

With perchloric acid; In acetic acid; acetonitrile;

DOI:10.1007/BF01166335

Reference yield: 75.0%

3-bromo-5-(4-bromophenyl)isoquinoquinazolinium perchlorate (173347-57-4) → C44H24Br4N4(2+)*2ClO4(1-)

Guidance literature:

In benzonitrile; for 0.5h; Reflux;

DOI:10.1007/s10593-008-0049-x

upstream raw materials:

(2-bromomethylphenyl)acetonitrile

Downstream raw materials:

3-bromo-(4-bromophenyl)-12H-isoquino[2,3-a]quinazoline