5-chloro-2-phenyl>-2'-fluorobenzophenone

Base Information

Chemical Name:5-chloro-2-phenyl>-2'-fluorobenzophenone
CAS No.:81537-96-4
Molecular Formula:C₂₂H₁₉ClFNO
Molecular Weight:367.85
Hs Code.:

5-chloro-2-<o-<(dimethylamino)methyl>phenyl>-2'-fluorobenzophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-chloro-2-phenyl>-2'-fluorobenzophenone

Chemical Property:

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Technology Process of 5-chloro-2-phenyl>-2'-fluorobenzophenone

There total 6 articles about 5-chloro-2-phenyl>-2'-fluorobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-12-1
4-chloromethoxybenzene

: 81537-96-4
5-chloro-2-phenyl>-2'-fluorobenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) 0 deg C, 25 h, ether/hexane, 2.) -12 to -5 deg C, 20 h

With n-butyllithium;
DOI:10.1021/jo00140a013

Reference yield:

: 82374-06-9
(3-chloro-6-methoxyphenyl)(2-fluorophenyl)methanone

: 81537-96-4
5-chloro-2-phenyl>-2'-fluorobenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / TiCl₄ / toluene / 40 h / Ambient temperature

With titanium tetrachloride; In toluene;
DOI:10.1021/jo00140a013

Reference yield:

: 393-52-2
2-Fluorobenzoyl chloride

: 81537-96-4
5-chloro-2-phenyl>-2'-fluorobenzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 87.5 percent / AlCl₃ / CH₂Cl₂ / 48 h / -10 - -5 °C

2: 93 percent / TiCl₄ / toluene / 40 h / Ambient temperature

With aluminium trichloride; titanium tetrachloride; In dichloromethane; toluene;
DOI:10.1021/jo00140a013