dichloro(2-tert-butyl-6-[(cyclohexylimino)methyl]phenolato)(η5-cyclopentadienyl)titanium

Base Information

Chemical Name:dichloro(2-tert-butyl-6-[(cyclohexylimino)methyl]phenolato)(η5-cyclopentadienyl)titanium
CAS No.:514791-67-4
Molecular Formula:C₂₂H₂₉Cl₂NOTi
Molecular Weight:442.264
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dichloro(2-tert-butyl-6-[(cyclohexylimino)methyl]phenolato)(η5-cyclopentadienyl)titanium

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Technology Process of dichloro(2-tert-butyl-6-[(cyclohexylimino)methyl]phenolato)(η5-cyclopentadienyl)titanium

There total 1 articles about dichloro(2-tert-butyl-6-[(cyclohexylimino)methyl]phenolato)(η5-cyclopentadienyl)titanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 215033-70-8
N-(3-tert-butyl-2-hydroxy)benzylidenecyclohexylamine

: 514791-67-4
dichloro(2-tert-butyl-6-[(cyclohexylimino)methyl]phenolato)(η5-cyclopentadienyl)titanium

Guidance literature:: With n-butyl lithium; In tetrahydrofuran; hexane; byproducts: LiCl; under N2; n-BuLi in hexanes added dropwise to stirred soln. of ligand inTHF (-78°C); stirred (30 min); warmed to room temp. for 1 h; coo led to -78°C; Ti complex added; held at -78°C for 1 h; warmed to room temp.; stirred overnight; solvent removed under vac.; extd. with CH2Cl2; concd.; layered with light petroleum; cooled to 5°C; elem. anal.;
DOI:10.1016/S0022-328X(02)02106-X