C₂₅H₄₅N₇O₆

Base Information

Chemical Name:C₂₅H₄₅N₇O₆
CAS No.:1367370-68-0
Molecular Formula:C₂₅H₄₅N₇O₆
Molecular Weight:539.676
Hs Code.:

C<sub>25</sub>H<sub>45</sub>N<sub>7</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₅H₄₅N₇O₆

Chemical Property:

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Technology Process of C₂₅H₄₅N₇O₆

There total 5 articles about C₂₅H₄₅N₇O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187839-36-6
C₁₆H₂₆N₆O₄

: 1367370-68-0
C₂₅H₄₅N₇O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / acetonitrile / 72 h / Inert atmosphere

2.1: palladium on activated charcoal; hydrogen / methanol

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

3.2: 48 h / 0 - 20 °C / Inert atmosphere

4.1: palladium on activated charcoal; hydrogen / methanol

With palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1039/c2cc00060a

Reference yield:

: 1187839-02-6
N₃(α-aminoisobutyric acid)₄OtBu

: 1367370-68-0
C₂₅H₄₅N₇O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / Inert atmosphere

2.1: acetic anhydride / 2 h / 120 °C / Inert atmosphere

3.1: triethylamine / acetonitrile / 72 h / Inert atmosphere

4.1: palladium on activated charcoal; hydrogen / methanol

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

5.2: 48 h / 0 - 20 °C / Inert atmosphere

6.1: palladium on activated charcoal; hydrogen / methanol

With palladium on activated charcoal; hydrogen; acetic anhydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1039/c2cc00060a

Reference yield:

: 1367370-64-6
N₃-(Aib)4-GlyNH₂

: 1367370-68-0
C₂₅H₄₅N₇O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium on activated charcoal; hydrogen / methanol

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

2.2: 48 h / 0 - 20 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / methanol

With palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1039/c2cc00060a