C₉H₇FOS

Base Information

• Chemical Name: C₉H₇FOS
• CAS No.: 1135283-78-1
• Molecular Formula: C₉H₇FOS
• Molecular Weight: 182.218
• Hs Code.: 2934999090
• Mol file: 1135283-78-1.mol

Synonyms:

Chemical Property of C₉H₇FOS

Chemical Property:

• Melting Point: 65-67°
• Boiling Point: 327.6±27.0 °C(Predicted)
• PKA: 13.66±0.10(Predicted)
• Density: 1.390±0.06 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

(7-Fluoro-1-benzothiophen-2-yl)methanol >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₇FOS

There total 1 articles about C₉H₇FOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 7-fluorobenzo[b]thiophene-2-carboxylate → C9H7FOS (1135283-78-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

C9H7FOS (1135283-78-1) → C24H21ClFNO4S

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 20 °C

2.1: sodium iodide / tetrahydrofuran / 0.5 h / 0 °C

2.2: 4 h / 20 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; potassium fluoride / N,N-dimethyl-formamide / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; potassium fluoride; N-Bromosuccinimide; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;

Refernces