(R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol

Base Information

Chemical Name:(R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol
CAS No.:195324-78-8
Molecular Formula:C₂₁H₂₆O₂
Molecular Weight:310.436
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol

Chemical Property:

Purity/Quality:

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Technology Process of (R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol

There total 9 articles about (R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73770-45-3
(R)-(+)-7,7-dimethoxy-5-(1-methylethenyl)-2-heptanone

: 195324-78-8
(R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol

Guidance literature:: Multi-step reaction with 9 steps

1: 68 percent / 9-BBN, H₂O₂

2: 81 percent / NaH

3: pyridine / 0 °C

4: potassium tert-butoxide / 2-methyl-propan-2-ol / 60 °C

5: 3N HCl / acetone

6: 2.) PCC, 3.) K₂CO₃

7: 85 percent / p-TsOH

8: 90 percent / acetonitrile / 1.5 h / 0 °C / Irradiation

9: 1.) BF₃*Et₂O, 2.) conc. HCl

With pyridine; hydrogenchloride; 9-borabicyclo[3.3.1]nonane dimer; boron trifluoride diethyl etherate; potassium tert-butylate; dihydrogen peroxide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0040-4039(97)21374-2

Reference yield:

: 195324-73-3
(R)-3-(2,2-Dimethoxy-ethyl)-2-methyl-heptane-1,6-diol

: 195324-78-8
(R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / NaH

2: pyridine / 0 °C

3: potassium tert-butoxide / 2-methyl-propan-2-ol / 60 °C

4: 3N HCl / acetone

5: 2.) PCC, 3.) K₂CO₃

6: 85 percent / p-TsOH

7: 90 percent / acetonitrile / 1.5 h / 0 °C / Irradiation

8: 1.) BF₃*Et₂O, 2.) conc. HCl

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; potassium tert-butylate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0040-4039(97)21374-2

Reference yield:

: 195324-75-5
(R)-3-(2-Benzyloxy-1-methyl-ethyl)-hept-6-enal

: 195324-78-8
(R)-7-(2-Benzyloxy-1-methyl-ethyl)-1-methyl-5,6,7,8-tetrahydro-naphthalen-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) PCC, 3.) K₂CO₃

2: 85 percent / p-TsOH

3: 90 percent / acetonitrile / 1.5 h / 0 °C / Irradiation

4: 1.) BF₃*Et₂O, 2.) conc. HCl

With hydrogenchloride; boron trifluoride diethyl etherate; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In acetonitrile;
DOI:10.1016/S0040-4039(97)21374-2