C₁₁H₁₂BrCl₂NO₂*BrH

Base Information

Chemical Name:C₁₁H₁₂BrCl₂NO₂*BrH
CAS No.:1452587-02-8
Molecular Formula:BrH*C₁₁H₁₂BrCl₂NO₂
Molecular Weight:421.944
Hs Code.:

C<sub>11</sub>H<sub>12</sub>BrCl<sub>2</sub>NO<sub>2</sub>*BrH

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Chemical Property of C₁₁H₁₂BrCl₂NO₂*BrH

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Technology Process of C₁₁H₁₂BrCl₂NO₂*BrH

There total 5 articles about C₁₁H₁₂BrCl₂NO₂*BrH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1452587-02-8
C₁₁H₁₂BrCl₂NO₂*BrH

Guidance literature:: Multi-step reaction with 5 steps

1: chlorine / acetic acid; water

2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

3: bromine / chloroform / 2 h / 20 °C

4: chloroform / 18 h / 20 °C

5: hydrogen bromide; water / methanol / 48 h

With water; hydrogen bromide; bromine; chlorine; potassium carbonate; In methanol; chloroform; water; acetic acid; N,N-dimethyl-formamide; 4: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 17044-70-1
3',5'-dichloro-4'-hydroxyacetophenone

: 1452587-02-8
C₁₁H₁₂BrCl₂NO₂*BrH

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

2: bromine / chloroform / 2 h / 20 °C

3: chloroform / 18 h / 20 °C

4: hydrogen bromide; water / methanol / 48 h

With water; hydrogen bromide; bromine; potassium carbonate; In methanol; chloroform; N,N-dimethyl-formamide; 3: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 1452587-06-2
C₁₁H₁₁BrCl₂O₂

: 1452587-02-8
C₁₁H₁₂BrCl₂NO₂*BrH

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / chloroform / 2 h / 20 °C

2: chloroform / 18 h / 20 °C

3: hydrogen bromide; water / methanol / 48 h

With water; hydrogen bromide; bromine; In methanol; chloroform; 2: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2013.07.017