C₂₃H₃₁BN₆O₈

Base Information

Chemical Name:C₂₃H₃₁BN₆O₈
CAS No.:1534328-73-8
Molecular Formula:C₂₃H₃₁BN₆O₈
Molecular Weight:530.346
Hs Code.:

C<sub>23</sub>H<sub>31</sub>BN<sub>6</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₂₃H₃₁BN₆O₈

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Technology Process of C₂₃H₃₁BN₆O₈

There total 6 articles about C₂₃H₃₁BN₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1534328-70-5
C₂₁H₂₁BrN₂O₈

: 1534328-73-8
C₂₃H₃₁BN₆O₈

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / dichloromethane; 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

4: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja411547j

Reference yield:

: 1534328-71-6
C₂₄H₃₄BrN₃O₇

: 1534328-73-8
C₂₃H₃₁BN₆O₈

Guidance literature:: Multi-step reaction with 3 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / dichloromethane; 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

3: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; triethylamine; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja411547j

Reference yield:

: 6940-50-7
4-bromo-DL-mandelic acid

: 1534328-73-8
C₂₃H₃₁BN₆O₈

Guidance literature:: Multi-step reaction with 6 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dmap / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: pyridine; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / dichloromethane; 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

6: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With pyridine; dmap; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja411547j