[Cu(I)(tris[2-(dimethylamino)ethyl]amine)(PPh₃)][BPh₄]

Base Information

• Chemical Name: [Cu(I)(tris[2-(dimethylamino)ethyl]amine)(PPh₃)][BPh₄]
• CAS No.: 1309874-42-7
• Molecular Formula: C₂₄H₂₀B*C₃₀H₄₅CuN₄P
• Molecular Weight: 875.468
• Mol file: 1309874-42-7.mol

Synonyms:

Chemical Property of [Cu(I)(tris[2-(dimethylamino)ethyl]amine)(PPh₃)][BPh₄]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [Cu(I)(tris[2-(dimethylamino)ethyl]amine)(PPh₃)][BPh₄]

There total 1 articles about [Cu(I)(tris[2-(dimethylamino)ethyl]amine)(PPh₃)][BPh₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tetrakis(acetonitrile)copper(I) perchlorate (14057-91-1) + tris[2-(dimethylamino)ethyl]amine (33527-91-2) + sodium tetraphenyl borate (143-66-8) + triphenylphosphine (603-35-0) → [Cu(I)(tris[2-(dimethylamino)ethyl]amine)(PPh3)][BPh4] (1309874-42-7)

Guidance literature:

In methanol; under Ar; Cu complex and PPh3 dissolved in MeOH; ligand added; NaBPh4 added; left at -35°C overnight; solvent removed; dissolved in acetone; crystd. by slow diffusion of Et2O; elem. anal.;

DOI:10.1039/c1dt10189g

upstream raw materials:

tetrakis(acetonitrile)copper(I) perchlorate

tris[2-(dimethylamino)ethyl]amine

sodium tetraphenyl borate

triphenylphosphine