hexakis-(trimethylsilyl)disilagermirane

Base Information

• Chemical Name: hexakis-(trimethylsilyl)disilagermirane
• CAS No.: 156628-39-6
• Molecular Formula: C₁₈H₅₄GeSi₈
• Molecular Weight: 567.901

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Chemical Property of hexakis-(trimethylsilyl)disilagermirane

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Technology Process of hexakis-(trimethylsilyl)disilagermirane

There total 1 articles about hexakis-(trimethylsilyl)disilagermirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

germanium(II) chloride-dioxane complex + (thf)3LiSi(SiMe3)3 → tris(trimethylsilyl)germane (104164-54-7) + hexakis(trimethylsilyl)digermane (104164-57-0) + tetrachlorotetrakis(tris(trimethylsilyl)germyl)cyclotetragermane + hexakis-(trimethylsilyl)disilagermirane (156628-39-6) + tetrakis(trimethylsilyl)germanium (19372-30-6)

Guidance literature:

In hexane; Ar-atmosphere; stirring at -78°C for 9 h, warming to room temp., stirring for 15 h; solvent removal (vac.), stirring with pentane for 1 h, filtration, evapn., repeated recrystn.;

DOI:10.1021/ic970833z

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