1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene

Base Information

Chemical Name:1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene
CAS No.:223114-70-3
Molecular Formula:C₁₈H₁₉BCl₂FeSn
Molecular Weight:491.623
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene

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Technology Process of 1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene

There total 3 articles about 1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 70595-34-5
1,1'-bis(trimethylstannyl)ferrocene

: 873-51-8
phenylborondichloride

: 223114-70-3
1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene

Guidance literature:: In further solvent(s); react. with 2 equiv. BCl3 in hexanes at -78°C, slow warming to room temp.; recrystn. (hexanes, -55°C); elem. anal.;

Reference yield: 31.0%

: 70595-34-5
1,1'-bis(trimethylstannyl)ferrocene

: 873-51-8
phenylborondichloride

: 223114-70-3
1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene

: 473544-64-8
1-chlorodimethylstannyl-3-chloro(phenyl)borylferrocene

Guidance literature:: In toluene; a soln. of C6H5BCl2 in toluene was added dropwise to a soln. of complex in toluene at -78°C, allowed to warm to ambient temp. and stirredfor 2 days (N2); volatiles were removed under reduced pressure (1E-3 Torr), kept under dynamic vac. at ambient temp. over 12 h, dissolved in hexane, filtered, evapd., recrystd. at -78°C from hexane;
DOI:10.1021/om0204890

Reference yield:

: 70595-34-5
1,1'-bis(trimethylstannyl)ferrocene

: 873-51-8
phenylborondichloride

: 223114-70-3
1-chlorodimethylstannyl-2-chloro(phenyl)borylferrocene

: 223114-56-5
1-trimethylstannyl-2-chloro(phenyl)borylferrocene

Guidance literature:: In further solvent(s); react. with 1 equiv. BCl2Ph in hexanes at -78°C, slow warming to 0°C, removal of volatiles (high vac.);